Mechanochemical recrystallization: Forgotten basics and new possibilities
نویسندگان
چکیده
The task of this article is to update, develop and introduce into scientific practice the method "mechanochemical recrystallization" in solid-phase systems with small additives liquid phase solvent precursors stabilize formed nanoparticles. essence shown using example mechanical activation S–AgNO3–NH4X system, where X = Cl, Br, I, addition dimethyl sulfoxide (DMSO), resulting mechanochemical synthesis sulfur-containing nanocomposites S/AgX controlled content sulfur nanoparticles (nanosulfur). predetermined nanosulfur ensured by a continuous process dissolution-crystallization (recrystallization) starting DMSO medium reactor. proposed technical solution made it possible obtain single treatment powder – AgNO3, NH4Х, NH4NO3 (diluent), commercial planetary ball mills various milling tools. also includes washing water-soluble components mechanosynthesis.
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ژورنال
عنوان ژورنال: Chimica techno acta
سال: 2023
ISSN: ['2411-1414', '2409-5613']
DOI: https://doi.org/10.15826/chimtech.2023.10.2.13